3-Nitrophthalic acid Basic information |
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3-Nitrophthalic acid Chemical Properties |
Melting point |
210 °C (dec.) (lit.) |
Boiling point |
350.79°C (rough estimate) |
density |
1.6342 (rough estimate) |
vapor density |
7.3 (vs air) |
refractive index |
1.5282 (estimate) |
storage temp. |
Refrigerator |
solubility |
water: soluble5%, clear to slightly hazy, colorless to faint yellow or tan |
pka |
pK1:1.88 (25°C) |
form |
Powder |
color |
Off-white to light yellow |
Water Solubility |
20 g/L (25 ºC) |
Decomposition |
216 °C |
BRN |
2054269 |
Stability: |
Stable. Incompatible with strong oxidizing agents. |
InChIKey |
KFIRODWJCYBBHY-UHFFFAOYSA-N |
CAS DataBase Reference |
603-11-2(CAS DataBase Reference) |
NIST Chemistry Reference |
3-Nitrophthalic acid(603-11-2) |
EPA Substance Registry System |
3-Nitrophthalic acid (603-11-2) |
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3-Nitrophthalic acid Usage And Synthesis |
Chemical Properties |
pale yellow crystals |
Synthesis Reference(s) |
The Journal of Organic Chemistry, 39, p. 2468, 1974 DOI: 10.1021/jo00930a051 |
Safety Profile |
A preparative hazard. When heated to decomposition it emits toxic fumes of NOx. |
Purification Methods |
Crystallise 3-nitrophthalic acid from hot water (1.5mL/g). Dry it in air. The amide has m 201o (from EtOH). [Beilstein 9 H 823, 9 IV 3275.] |
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3-Nitrophthalic acid Preparation Products And Raw materials |
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