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Cinnamoyl chloride Basic information |
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Cinnamoyl chloride Chemical Properties |
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Cinnamoyl chloride Usage And Synthesis |
Chemical Properties |
white to yellowish crystalline solid |
Uses |
Titrimetric determination of small amounts of water. |
Synthesis Reference(s) |
Organic Syntheses, Coll. Vol. 3, p. 714, 1955
Tetrahedron Letters, 14, p. 5121, 1973 DOI: 10.1016/S0040-4039(01)87403-7 |
Hazard |
Skin irritant. |
Purification Methods |
Refractionate it in a vacuum until the distillate solidifies on cooling, and recrystallise it from pet r. The trans-amide has m 145-150o (from H2O) [Beilstein 9 III 2711]. [Adams & Ulich J Am Chem Soc 42 605 1920, Bergmann et al. J Chem Soc 2524 1952, Beilstein 9 H 587, 9 I 233, 9 II 390, 9 III 2710, 9 IV 2020.] |
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Cinnamoyl chloride Preparation Products And Raw materials |
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